Synthesis, NMR spectroscopic and X-ray crystallographic studies of N-acetyl-3-butanoyltetramic acid

 
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Journal part (EN)
Scientific article (EN)
1994 (EN)
Synthesis, NMR spectroscopic and X-ray crystallographic studies of N-acetyl-3-butanoyltetramic acid (EN)
Barkley, JV (EN)
Markopoulou, O (EN)
Markopoulos, J (EN)
The reaction of N-acetylglycine p-nitrophenyl ester with the anion of an active methylene compound proceeds to give N-acetyl-3-butanoyltetramic acid. The influence of the N-acetyl group on the equilibrium between different 'internal' and 'external' tautomeric forms of N-acetyl-3-butanoyltetramic acid was investigated by H-1 and C-13 NMR spectroscopy. The structure of this compound was confirmed by an X-ray crystal structure determination. (EN)
journalArticle (EN)
Chemistry, Organic (EN)
ACTIVE METHYLENE-COMPOUNDS (EN)
3-ACYLTETRAMIC ACIDS (EN)
COMPLEXES (EN)
ACYLAMINOACETYL DERIVATIVES (EN)
IKARUGAMYCIN (EN)
PYRROLIDINE-2,4-DIONES (EN)
(+)-IKARUGAMYCIN (EN)
SUBSTITUTED TETRAMIC ACIDS (EN)
Chemistry, Physical (EN)
METABOLITE (EN)
CYCLIZATION (EN)
National Technical University of Athens
Digital Library of National Technical University of Athens | Dspace@NTUA
Κεντρική Βιβλιοθήκη Ε.Μ.Π.
Ιδρυματικό Αποθετήριο
Δημοσιεύσεις μελών Δ.Ε.Π. σε περιοδικά
Journal of the Chemical Society, Perkin Transactions 2 (EN)
English
1994 (EN)
http://hdl.handle.net/123456789/11363
6 (EN)
0300-9580 (EN)
ISI:A1994NQ34100024 (EN)
1274 (EN)
1271 (EN)
ROYAL SOC CHEMISTRY (EN)



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